TOC analytical method in cleaning validations: criteria, limits and robustness of the process
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| Model | Automatic Organic Halogen Analyzer Model AOX-400 |
| Application measures | River water, industrial effluents, soil, etc. |
| Sample types | Solid (AOX: aqueous liquid sample adsorbed on activated carbon).
Liquid (EOX: extraction) |
| Method of analysis | Oxidative pyrolysis / Columbiometry |
| Oven temperature | 300 – 1000 °C (recommended 950 °C |
| Introduction shows | Introduction through the open top of the combustion tube.
AOX: Injection of the sample with the activated carbon in the column through a punch (column method). Introduction of the frit with the sample adsorbed on the activated carbon (Stirring method). EOX: Direct injection with syringe |
| Range measured | Total Organic Halogens: 0.1 to 50 μg |
| Sample quantity | Samples AOX: 50 mg approx, EOX: Less than 200 μl |
| Measurement time | Less than 10 min/measurement (for 2 μg values) |
| Number of samples | Frit: 30 samples Column: 60 samples
EOX: 40 samples (Size 2 mL vials with septum) |
| Gas | Using AIR200, no cylinder air supply is required AOX: Air (800 ml/min)
ECOX: Air (100 ml/min) + Oxygen (300 ml/min) |
| Working conditions | 15 to 35 °C, below 75% humidity (non-condensing) |
| Power supply | AC 100/115/230/240 V, 50/60 Hz, 960 VA |
| Dimensions Weight | AOX-400: Approx. 460 x 420 x 560 mm (width x depth x height) / approx. 37 Kg
SI-400: Approx. 200 x 305 x 410 mm (W x D x H) / approx. 7 kg (7 lbs.) AIR-200: Approx. 100 x 400 x 220 mm (width x depth x height) / approx. 5 Kg |
| Data control devices | PC compatible with Windows ® |
Sampler:
| Stirring method | Set Frits |
| Column method | SI-400 + set columns |
| EOX | SI-400 + EOX set |
ISO 9562
DIN EN 1485
EPA 9020
DIN 38414-H1
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